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Precision crystallization, Leubner, Ingo


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Автор: Leubner, Ingo
Название:  Precision crystallization
ISBN: 9780367385163
Издательство: Taylor&Francis
Классификация:

ISBN-10: 0367385163
Обложка/Формат: Paperback
Страницы: 216
Вес: 0.91 кг.
Дата издания: 19.09.2019
Язык: English
Размер: 156 x 234 x 12
Читательская аудитория: Tertiary education (us: college)
Подзаголовок: Theory and practice of controlling crystal size
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Поставляется из: Европейский союз
Описание:

Despite the fact that crystals make up an estimated 80% of chemical and pharmaceutical products, few resources exist that provide practical guidance on achieving precision control of their size and size distribution. Based on a model developed by the author and his colleagues, Precision Crystallization: Theory and Practice of Controlling Crystal Size presents scientists and product engineers with the tools to control crystal nucleation, enabling them to ultimately control crystal size and size distribution for batch and continuous crystallizations.





At the cutting edge of crystallization science and technology, this volume presents information never before available. Introducing the Balanced Nucleation and Growth (BNG) model, the book demonstrates how the results of the nucleation process are quantitatively related to practical experimental control values such as:









  • reaction addition rate


  • crystal solubility


  • temperature


  • residence time (continuous crystallizations)


  • the effect of ripening agents (crystal supersizing) during nucleation


  • the effect of crystal growth restrainers (crystal nanosizing) during nucleation


  • control of renucleation






The author shows how the BNG theory predicts previously unknown phenomena and also how it corrects erroneous perceptions of the importance of reaction volume on the outcome of crystal nucleation. Going above and beyond classical nucleation theories which rely to a large extent on guesswork, the BNG model gives precise guidance to scientists working in a range of critical areas, leading to promising implications for research, quality control, product development, production processes, pilot plant operations, and manufacturing.



Membrane-Assisted Crystallization Technology

Автор: Drioli Enrico, Di Profio Gianluca & Curcio Efrem
Название: Membrane-Assisted Crystallization Technology
ISBN: 1783263318 ISBN-13(EAN): 9781783263318
Издательство: World Scientific Publishing
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Цена: 14890.00 р.
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Описание:

This book covers all the basic and applied aspects of crystallization processes based on membrane technology. Synthesis and processing of membrane materials are discussed and reviewed, while mass/heat transport and control are treated in view of the non-reversible thermodynamic principles and statistical thermodynamics. Engineering process design and crystalline materials products properties, and also the relation to other traditional crystallization formats, are analyzed. Advantages, limitations, and future developments are also included in the content, with special emphasis on new fields of applications like microfluidic configurations, controlled proteins (also membrane proteins) crystallization, organic semiconductors single crystals production, and optical materials.

From Molecules to Crystallizers: An Introduction to Crystallization

Автор: Garside, John;Davey, Roger (both of the Chemical E
Название: From Molecules to Crystallizers: An Introduction to Crystallization
ISBN: 0198504896 ISBN-13(EAN): 9780198504894
Издательство: Oxford Academ
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Цена: 5226.00 р.
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Описание: Crystallization is one of the oldest separation processes used in the chemical industry and is still one of the most important. The proposed primer will emphasize the link between a process engineering description of crystallizer design and operation and provide a thorough molecular level understanding of the kinetics of nucleation and crystal growth and of habit modification and polymorphism.

Industrial Crystallization

Автор: Lewis
Название: Industrial Crystallization
ISBN: 1107052157 ISBN-13(EAN): 9781107052154
Издательство: Cambridge Academ
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Цена: 10771.00 р.
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Описание: A comprehensive overview of the theory and practice of industrial crystallization. Providing new industry-relevant information that has not been published before, and supported by real world case studies and worked examples, this is an ideal resource for students and industry practitioners alike.

Crystallization Handbook

Автор: Hollis Garry
Название: Crystallization Handbook
ISBN: 1632381044 ISBN-13(EAN): 9781632381040
Издательство: Неизвестно
Цена: 24943.00 р.
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Industrial Crystallization

Автор: Narayan S. Tavare
Название: Industrial Crystallization
ISBN: 148990235X ISBN-13(EAN): 9781489902351
Издательство: Springer
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Цена: 28734.00 р.
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Описание: Incorporating all recent developments and applications of crystallization technology, this volume offers a clear account of the field`s underlying principles, reviews of past and current research, and provides guidelines for equipment and process design.

The Effects of Ultrasound on the Kinetics of Crystallization

Автор: Alexander P. Kapustin
Название: The Effects of Ultrasound on the Kinetics of Crystallization
ISBN: 1468415506 ISBN-13(EAN): 9781468415506
Издательство: Springer
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Цена: 13060.00 р.
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Описание: an ultra- 6 2 sound flux as low as 10 W/cm at 3 x 10 cis produces a pressure wave whose amplitude is 5 atm, while the 5 maximum acceleration may exceed 10 times that of gravity, the maximum particle speed being 40 m/sec and 2 the radiation pressure 1300 dynes/cm [I, 2].

Spherical Crystallization as a New Platform for Particle Design Engineering

Автор: Yoshiaki Kawashima
Название: Spherical Crystallization as a New Platform for Particle Design Engineering
ISBN: 981136785X ISBN-13(EAN): 9789811367854
Издательство: Springer
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Цена: 23757.00 р.
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Описание:

This book describes the principles and applications of the spherical crystallization technique, from the standpoint of its inventor. After an introduction on the history of particle design engineering and nanotechnology, the concept of spherical crystallization itself is clearly explained. Attention then turns to the application of spherical crystallization in pharmaceutical processes. It is explained how the technique can provide physicochemical properties suitable for direct tableting of active pharmaceutical ingredients and how it has enabled the development of a novel particulate design platform from single to complex system. Subsequent chapters describe the roles of polymeric spherical crystallization in the preparation of novel microspheres, microballoons for drug delivery systems (DDS) and the development of biocompatible and biodegradable poly(D,L-lactide-co-glycolide) (PLGA) nanospheres. The various applications of PLGA nanospheres composite within oral-, pulmonary-, transdermal DDS and cosmetics are fully discussed. Finally, future perspectives are presented on use of the technology in the design and industrial-scale manufacture of new drug delivery systems, highlighting how a continuous pharmaceutical process that meets US Food and Drug Administration quality requirements should soon be introduced.
Industrial Crystallization

Автор: Narayan S. Tavare
Название: Industrial Crystallization
ISBN: 0306448610 ISBN-13(EAN): 9780306448614
Издательство: Springer
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Цена: 36570.00 р.
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Описание: Incorporating all recent developments and applications of crystallization technology, this volume offers a clear account of the field`s underlying principles, reviews of past and current research, and provides guidelines for equipment and process design.

Crystallization of Nanoscaled Colloids

Автор: Philip G. Born
Название: Crystallization of Nanoscaled Colloids
ISBN: 3319032968 ISBN-13(EAN): 9783319032962
Издательство: Springer
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Цена: 14365.00 р.
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Описание: Exploring processes that create ordered assemblies from disordered nanoparticles, this work examines the self-assembly of particles, a process widely employed, but not yet well understood. Offers new models describing the competition of different influences.

Crystallization Modalities in Polymer Melt Processing

Автор: Hermann Janeschitz-Kriegl
Название: Crystallization Modalities in Polymer Melt Processing
ISBN: 3709117496 ISBN-13(EAN): 9783709117491
Издательство: Springer
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Цена: 18284.00 р.
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Описание: This book is the first to explicitly focus on the processing of crystallizing polymers. It is also the first to address the unexpectedly strong interaction of three transport phenomena: heat transfer, momentum transfer (rheology) and crystalline kinetics.

Crystallization Processes under Hydrothermal Conditions

Автор: A. N. Lobachev
Название: Crystallization Processes under Hydrothermal Conditions
ISBN: 1468475258 ISBN-13(EAN): 9781468475258
Издательство: Springer
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Цена: 13060.00 р.
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Описание: This collection conta ins the results of a number of investiga- tions which have been carried out in the Hydrothermal Synthesis Laboratory of the Institute of Crystallography, Academy of Sciences of the USSR;

Interphases and Mesophases in Polymer Crystallization II

Автор: Giuseppe Allegra; A. Abe; . Auriemma; S. Bracco; A
Название: Interphases and Mesophases in Polymer Crystallization II
ISBN: 3642064655 ISBN-13(EAN): 9783642064654
Издательство: Springer
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Цена: 32651.00 р.
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Описание: 1 F. Auriemma, C. De Rosa, P. Corradini: Solid Mesophases in Semicrystalline Polymers: Structural Analysis by Diffraction Techniques.- 2 L. Li, W.H. de Jeu: Flow-Induced Mesophases in Crystallizable Polymers.- 3 A. Abe, H. Furuya, Z. Zhou, T. Hiejima, Y. Kobayashi: Stepwise Phase Transitions of Chain Molecules: Crystallization/Melting via a Nematic LC Phase.- 4 P. Sozzani, S. Bracco, A. Comotti, R. Simonutti: Motional Phase Disorder of Polymer Chains as Crystallized to Hexagonal Lattices.-


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