Joseph Goldstein; Dale Newbury; David Joy; Joseph Scanning Electron Microscopy and X-Ray Microanalysis 9781493966745

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Автор: Joseph Goldstein; Dale Newbury; David Joy; Joseph
Название: Scanning Electron Microscopy and X-Ray Microanalysis
Перевод названия: Джозеф Голдштейн: Сканирование электронным микроскопом и микроанализ с помощью X-лучей
ISBN: 9781493966745
Издательство: Springer
Классификация:

Наукометрия и системы индексов

Биофизика

Спектральный анализ, спектрохимия, масс-спектрометрия

Испытания материалов

ISBN-10: 149396674X
Обложка/Формат: Hardback
Страницы: 700
Вес: 1.79 кг.
Дата издания: 2017
Серия: Materials Science
Язык: English
Издание: 4 rev ed
Иллюстрации: 149 black & white illustrations, 397 colour illustrations, 348 colour tables, biography
Размер: 217 x 284 x 34
Читательская аудитория: Graduate/advanced undergraduate textbook
Ссылка на Издательство: Link
Рейтинг:
Поставляется из: Германии
Описание: This thoroughly revised and updated Fourth Edition of a time-honored text provides the reader with a comprehensive introduction to the field of scanning electron microscopy (SEM), energy dispersive X-ray spectrometry (EDS) for elemental microanalysis, electron backscatter diffraction analysis (EBSD) for micro-crystallography, and focused ion beams. Students and academic researchers will find the text to be an authoritative and scholarly resource, while SEM operators and a diversity of practitioners - engineers, technicians, physical and biological scientists, clinicians, and technical managers - will find that every chapter has been overhauled to meet the more practical needs of the technologist and working professional. In a break with the past, this Fourth Edition de-emphasizes the design and physical operating basis of the instrumentation, including the electron sources, lenses, detectors, etc.

In the modern SEM, many of the low level instrument parameters are now controlled and optimized by the microscopes software, and user access is restricted. Although the software control system provides efficient and reproducible microscopy and microanalysis, the user must understand the parameter space wherein choices are made to achieve effective and meaningful microscopy, microanalysis, and micro-crystallography. Therefore, special emphasis is placed on beam energy, beam current, electron detector characteristics and controls, and ancillary techniques such as energy dispersive x-ray spectrometry (EDS) and electron backscatter diffraction (EBSD).

With 13 years between the publication of the third and fourth editions, new coverage reflects the many improvements in the instrument and analysis techniques. The SEM has evolved into a powerful and versatile characterization platform in which morphology, elemental composition, and crystal structure can be evaluated simultaneously. Extension of the SEM into a dual beam platform incorporating both electron and ion columns allows precision modification of the specimen by focused ion beam milling.

New coverage in the Fourth Edition includes the increasing use of field emission guns and SEM instruments with high resolution capabilities, variable pressure SEM operation, theory, and measurement of x-rays with high throughput silicon drift detector (SDD-EDS) x-ray spectrometers. In addition to powerful vendor- supplied software to support data collection and processing, the microscopist can access advanced capabilities available in free, open source software platforms, including the National Institutes of Health (NIH) ImageJ-Fiji for image processing and the National Institute of Standards and Technology (NIST) DTSA II for quantitative EDS x-ray microanalysis and spectral simulation, both of which are extensively used in this work. However, the user has a responsibility to bring intellect, curiosity, and a proper skepticism to information on a computer screen and to the entire measurement process.

This book helps you to achieve this goal. Realigns the text with the needs of a diverse audience from researchers and graduate students to SEM operators and technical managersEmphasizes practical, hands-on operation of the microscope, particularly user selection of the critical operating parameters to achieve meaningful resultsProvides step-by-step overviews of SEM, EDS, and EBSD and checklists of critical issues for SEM imaging, EDS x-ray microanalysis, and EBSD crystallographic measurementsMakes extensive use of open source software: NIH ImageJ-FIJI for image processing and NIST DTSA II for quantitative EDS x-ray microanalysis and EDS spectral simulation. Includes case studies to illustrate practical problem solvingCovers Helium ion scanning microscopyOrganized into relatively self-contained modules - no need to read it all to understand a topicIncludes an online supplement-an extensive Database of Electron-Solid Interactions-which can be accessed on SpringerLink, in Chapter 3

Дополнительное описание: Goldstein et al., Scanning Electron Microscopy and X-Ray Microanalysis 4th ed.

Scanning Electron Microscopy and X-Ray Microanalysis, Joseph Goldstein; Dale Newbury; David Joy; Joseph